Phil Hamling 376 County Route 1 Warwick, NY, USA 10990 e-mail: pdah-at-optonline.net (change the -at- to @)
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Zinc Silicate Crystalline Glaze Pottery A chronicle of my recent progress and a way for me to keep it straight in my head! Click on thumbnails to enlarge photos |
Info I've been asked to keep in confidence. |
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11-12-08 I haven't been able to spend any meaningful time in the studio recently but here's a collection of interesting photos.
11-7-08 I ran into some old friends the other day and told them about the Crystalline Glaze Forum. They were all ears. Then I started describing all the people I've met and great times we've had. When I told them about this guy in western New York State whose studio is in a geodesic dome they loaded up and drove away chanting "We're off to see the Wizard, the wonderful Wizard of Koz". Here's a look at them driving down Pennsylvania Avenue.
11-6-08 Someone e-mailed me referencing my web page and asking questions about using a cone 6 kiln for firing crystals. I inadvertently deleted it before responding. If you read this can you re-send it? I'm happy to reply.
88th Firing Results
I was playing with my clear base with 2% titania, 4% copper carbonate, a fraction of cobalt carbonate and up to 5% Zircopax. I'm going have to sit with my notebook and see what it all means. I do think I will use a different schedule on the next loads. This one has 3 crash cools to ~850°C followed by gradual climbs to 1080°C. The crashes do give a sharp delineation between segments of the program but seem to nucleate way too many crystals
I'm starting to get it together to make the plaster models for casting some Christmas tree ornaments. |
Chattered Vase by Diane Luedemann. Click here for a plate |
Click here for more pics of the Hoppa's zincite |
October 25, 2008
Talk about jonesing! This is my first firing in 34 days. I finally got to spend an afternoon in the studio thanks to a rainy afternoon now that Crystalline Spectrum show, all those pesky home emergencies and the lawn care season are over. It should be smooth sailing for a while even though I still have to figure out who to vote for. It's gonna' be a tough choice.
88th Firing Setup |
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The Grasshopper asked me about seeding. Well....he wrote "Do you know a lot about seeding? If so, fill me in."
Well........................(Should I use more .....s Mr Wizard?).............I can say:
-Seeding helps maximize the number of crystals which grew throughout the full range of the crystal growth portion of the firing cycle.
-Very small pieces of zincite can nucleate crystals.
-If the pieces of zincite are too large you get bumps on the finished piece and often get those "ice cream cone", or "pointy leaf" shaped crystals.
-Fa showed us how to impress larger pieces of zincite in leather hard pots, but I don't like this method as much because it made those funky pointy bottom shaped crystals.
October 16, 2008 Mysterio Unveiled!
October 15, 2008 ..............................An Historic Perspective.............................
SEVRES |
More on Adelaide Alsop Robineau |
Bill Schran wrote: Subject: FW: Nice old picture of the Sevres plant with craftsman using a spray gun for glaze. Hey Phil, Wonder if this is a shot of the guy spraying crystal glaze? Bill http://cgi.ebay.com/ws/eBayISAPI.dll?ViewItem&item=250307931191&ssPageName=A |
October 12, 2008 I haven't been able to spend much time in the studio but have been able to do some striking at 815°C (1500°F). Well I guess that's what you call it. I heated 400°C per hour to 815°C then held for 1/2 hour.
Other Recent Distractions
October 9, 2008 Photos from the Crystalline Spectrum thanks to Rod and Denise Simair.
October 1, 2008 Glaze Catcher Removal Notes
September 28, 2008
We stopped to see Paul Lorber at the Peter's Valley Craft Fair in Sussex, NJ after the Crystalline Spectrum show and traded for a beautiful piece. |
Back in the studio with the Wizard |
September 26 to 28, 2008 CRYSTALLINE SPECTRUM
Workshop | Exhibitors | Exhibition | Event |
September 23, 2008
CRYSTALLINE SPECTRUM Update Click here for my page
I got some shots from Dick White late last night showing the gallery almost set up. Click on the picture, or here, for a sneek preview. Yo Hoppa! I saw this logo on a piece of turf equipment and thought of you. |
September 22, 2008
86th Firing Results | 87th Firing Setup |
These pieces came out much better in that the crystals are much larger. There still isn't enough background though. I guess I should have put on even more glaze. There really wasn't that much more that showed up in the glazecatchers.
I am re-re-re-re-firing some of these in the 87th firing. I mixed a batch of 4% titania base and added 5% CMC to make a thick paste. I gobbed as much on as I thought would stay, kept track of how much weight of glaze I added this time and put them on extra catchers.
September 20, 2008
86th Firing Setup This is another refire. I added a layer of 8% rutile base to 2 pieces and a mixture of 8% rutile and 8% titania to the others. I've slowed down the cooling rate from top end from 800 to 200°C/hr. |
CRYSTALLINE SPECTRUM Update Click here for my page
The gallery being set up for the show. Bill Schran is moving so fast you can't even see him in the photo.
I do think I spot my pieces as well as work from Bill Campbell, Ginny Conrow, Jamie (The Wizard of Clay) Kozlowski and Robert Hessler.
Regarding my presentation on heating element design, I'll be scrambling to button it down early this week.
September 19, 2008 85th Firing Results: Refire of 84th Firing. I didn't add any additional glaze to these pieces before the refire.
Just call her Krystal Kat, striking a Heisman Trophy pose.
9-18-08 84th Firing Results | 9-17-08 Test Fire Re-Fire Re-Fire Result |
September 16, 2008
84th Firing Setup | Test Fire Re-Fire Re-Fire | Test Fire Re-Fire Results |
September 15, 2008
83rd Firing Results |
The best color is in the catcher |
Tonight's bisque. |
Test Fire Results | Test Fire Re-Fire |
September 14, 2008
September 11, 2008 I can't believe it's been 7 years already!
September 10, 2008
82nd Firing Setup - I glazed the first large form I made with .30 g/sq.in. glaze loading and put it in the kiln with my extended lid on. I don't think there is any risk of this lid popping open during firing. I hit the start button and ran (crawled) to bed. I will see the results late 9-11-08.
81st Firing Results - Having the lid firmly closed seems to be the key. Both cone packs had cone 11 touching and the glazes came out as expected.
September 9, 2008
When I got there this morning the unit was at 1269ºC on its way to 1290ºC. Just looking in the studio door I could see the lid was propped up 1/4" to 1/2" and leaking heat like crazy. I pushed the lid back down and saw the temperature climb. The program calls for a rate of rise of 185ºC / hr with a 20 minute hold. When it reached temperature I noticed the 2 ^9's were just beginning to bend. After 10 minutes worth of soak ^10 was almost touching and ^11 was on it's way down. I see these cones fall pretty quickly. I never watched them before. I have no doubt ^11 will be touching when I get to check it tonight.
Most likely what happened in the previous firing is that the lid was propped open even more and it did take longer to get to top temperature (even it it was just by 20 minutes I can see how it would make a difference). This would explain why the room was so darned hot (100ºF) which I've never seen before
In chasing what may have happened I got input from the likes of William Melstrom, Avi Harrman, John Tiltion, Steve Lewicki, Rob Battey and Dave Bartlett. Suggestions included: 1) check the program, 2) inspect the elements, 3) clean the thermocouple connections, 4) verify various controller settings and 5) be there to witness what is happening when it reaches top end.
I did all these things.When I removed the tc extension wire and cleaned the ends with a Scotch Brite pad I didn't see much if any corrosion.
Mr Wizard.....Thank you so much for the input. After loading the kiln with a reglazed piece and cone paks I set the delay timer to 4 hours so I could be there when it hit top end this morning.
September 7, 2008
80th Firing Result - WTF????? I thought this was going to a rather mundane firing. It didn't turn out that way. I had a re-fire, 2 pieces with NFU at a low loading (~.35 g / sq. in.) and one piece with NFU + 1/2% cobalt carbonate, which should have yielded pieces with 1 1/2" to 2" dia. crystals. When I first peeked in I saw very few smallish crystals - not what I was expecting. It looked like an overfiring condition, but I have limited experience.
After closer examination I saw that ^11 had slumped well beyond where it had in the past (^11 touching). The first photo above shows ^'s 9, 10 & 11 from this firing in front and typical cones from previous firings in the rear. It looks more like ^13 to ^14 to me.
I'm in a quandry as to what to do to get back to the normal ^11 touching situation I've seen in the past. I checked the program and saw that nothing had changed. Is it a thermocouple degradation thing? Are they in need of replacement? I would expect platinum Rhodium thermocouples to last a very long time at this temperature. Is it just a "computer thing" and will rebooting the unit set it straight? I have many more pieces I was going to put this this routine firing, but don't want to screw them up and am not quite sure what to do.
Doll Test Firing Result - Well there certainly is some green showing but the pieces are all fish scaled. Even with a 30 minute hold at 1290ºC ^11 only came down to ~3 o'clock. I added another layer of uncolored 8% titania glaze to the pieces when they were still above 100ºC (it sticks prettty well) and refired it with a 35 minutes soak at the top end.
September 6, 2008
80th Firing Setup |
Doll Test Firing |
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A few more NFU pieces plus a refire. I'm using the schedule of 4-27-08 except I've sped up the first 3 segments |
2 refires plus a new one. All have some copper in hopes of having some nice stuff to reduce at Bill Schran's. |
September 4, 2008
September 1, 2008 Labor Day Holiday Weekend
August 30, 2008
Gettin' glaze catchers together. I'm going to stitch the split prismatic one on the seams with scrap platinum thermocouple wire. (Is that an oxymoron or what?) |
Kat got the itch to throw some pots. |
August 26, 2008
My latest attempt at making something of this form. |
More creations from Andy Boswell |
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These sunflowers have re-seeded themselves for several years now and are in peak bloom. |
Connie's Bunnies |
August 23, 2008 One more try!
Notes on Bill Schran's show
THE CRYSTALLINE SPECTRUM: A JOURNEY FROM STUDENT TO MASTER
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My current studio mate! |
It was glorious out in the yard today. The sun had that intensity which makes fresh cut grass glow. |
The Grasshopper's new stamp. Nice stuff Nathan! |
August 20, 2008
A bit of epoxy added to stand 'er up and I think I'm seeing a pot with a little attitude. |
Straight from the goose that laid the golden egg. Thanks a million Mr. Wizard! |
August 17, 2008
August 17, 2008
79th firing setup. Mostly NFU at .35 g/sq. in. loading |
Trying to make a little less of a "Pegleg Pete" this time. |
Kat & Dillon's camouflage paint job on the fountain controls. |
Increasing the hold time to 30 minutes brought ^11 close to touching, but there's nothing to write home about in terms of the glaze. I added 2 1/2 coats of fresh glaze and am firing them for the third time.
August 16, 2008
Not much background here. I'm re-firing these now. |
Avi, It survived the bisque and is ready for glaze. |
I increased the Doll's hold time at 1290C to 30 minutes in the hopes of getting ^11 touching in this test firing. Maybe that will help with fewer crystals.
August 13, 2008........Totally Off Topic
A contractor friend of mine has had a job building a Buddhist Temple recently. Pictured are 2 "doohickeys" he'll be installing soon. |
August 10, 2008
I have to tell you.....This is probably the most rewarding slab built form I've made yet. I really enjoyed the process and like the shape too. I'm sure it breaks many of the "Art" rules, but who cares. I like it. It's about 18 inches tall and I can't wait to see some nice crystalline rings on it. I plan to use NFU at a low loading rate where I'll see minimal glaze run off and have built a glaze catcher kind of doohickey into the base.
This is the kiln I recently bought from a friend for $120. He bought it off the sidewalk from a guy who was trying to get. Although it has strictly manual control I think it will be useful for use as a reduction torture machine. It looks like it is circa the 1970's to me. I'll have to check with Steve Lewicki to find out if the serial number helps date it. I'll bet its older than the Grasshopper.
The elements are in great shape and look like they have seen heat < 1/2 dozen times. The brick between sections was a little chewed up but I applied some ZIRCAR AX Moldable and CTP-1 Paper between the joints and they look to be sealed up right nice!
August 6, 2008
Nothing better than a fresh hair cut. |
It's amazing how much the weeping willows have recovered from their June 1st pruning. |
Don't tell anyone but Bella has a foot fetish. |
Tales from the Pickle Jar
This test involved using the same glaze*, on the same clay, in the same firing at different loading rates. (*OK, it had been aged 6, 23 and 65 days in a jar before I used it.) It appears aging (at least for this time period) makes no difference in the reaction of the glaze, but glaze thickness does not only with the color of the background but with the shape and color of the crystals. Note how little runoff there was from the pots with the lower glaze loadings.
The background color and shape of the brown crystals change significantly with glaze thickness. |
August 3, 2008
August 2, 2008
I have used Gorilla glue for years but never read the directions. It says to moisten one surface with water which causes the glue to foam. It works like a charm and makes the glue foam and harden in 4 hours. Being water based it doesn't dissolve the blue foam like Super 77 spray adhesive or other petroleum based material do. I'm going to put a bunch of material together an machine the forms on a CNC router this time.
July 30, 2008 - 77th Firing Results
July 26, 2008 - 77th Firing
July 29, 2008 |
July 28, 2008 |
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Sneak Preview -250°C | Setup |
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July 24, 2008 |
July 27, 2008 |
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The Wizard's Army | Glads | Bella, Bella, Bella! | DT reduction. |
Crystalline Glaze Quiz
Name the 5 frequent Crystalline Glaze Forum visitors who created these.
July 20, 2008
Fishing this weekend in NY's Thousand Islands
Phil won the bet with the 6#, 32" Northern Pike he took off Scow Island with Singer Castle on Dark Island visible across the shipping channel.
July 16, 2008 76th Firing Results
July 14, 2008 76th Firing Setup
July 13, 2008
The results of the 74th firing were poor (from a visual sense) to say the least. The crystals were quite bland and there was virtually no run off in the catcher. So I quickly loaded some more glaze on the bowl getting the loading up to .40 g/sq.in. On the positive side I did learn that a loading of .25 g of solids per sq. in of area just isn't enough. Also there were many, many pinholes. Then Mr. Turner told me, in an attempt to save electricity $, he bisqued these pieces to ^06 using the "Slow Glaze" cycle which runs much faster than the bisque cycles. My guess is the clay wasn't hot enough long enough to complete its dehydroxylation and off gassing.
July 12, 2008
The 17 1/2" dia. David Turner bowl in this firing has the glaze (NFU) brushed as thin as I could while getting a real even single coat. It worked out to be ~.25 g of solids per sq. in of area. This is about 1/2 the loading of June 16th's firing - a lighter loading than I expected. It is reproducible, and I can add more and keep track of exactly how much I have on as I'm glazing.
I expect this will give a look similar to the results of my 68th firing and will see for sure tonight (7-13-08). I plan to explore loadings in between .25 and .5 g solids per sq. in.
The kitchen is coming along real nice. We're hoping to pick out the granite counter tops this week. John Welch (www.finekitchenandbath.com) has been doing a fantastic job and is a pleasure to work with, plus I think he's more anal than I am, if that's possible! |
Patti modeling the spring loaded wiffle ball antennae earmuffs I made to add a little comedy to lawn mowing. |
This year's blueberry crop is looking real good! |
July 5, 2008
July 4, 2008
June 29, 2008
June 29, 2008
June 27, 2008
June 24, 2008
David, I'd say tonight's smoking was quite nice indeed. You really pulled out all the rings nicely. I wonder if a little iron would give some yellow highlights?
June 23, 2008
Shaped with wood putty and then 2 coats of latex paint. |
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Before and after 3X reduction by David Turner. |
June 16, 2008 73rd Firing Results
I'm still trying to get a good handle on the relationship of crystal growth to glaze thickness for this glaze when fired in the low temperature range (860C to 1000C). I brushed one heavy coat of the pudding consistency glaze on each piece with and additional 1 1/2" band on top.
For the 2 pieces in the right photo I measured the amount of glaze I added and estimated their surface area to determine the loading rate. They had 0.51 and 0.46 g solids / sq. in. of surface. All these have the characteristic look of some of the first NFU pieces I made. I can, and will, apply the glaze more thinly (0.4 g / in. sq.) on future pieces to hopefully get back to the "explosive" crystal growth I saw before.
Regarding the 2 pieces in the right photo, the one on the left had the 2 1/2 week old glaze and the one on the right had it from a new batch. I don't think the aged stuff worked as well.
June 15, 2008 Happy Father's Day!
A 2 1/2 week old "pickle jar" of NFU. |
73rd Firing Setup Thanks for the photos, Kat. |
Another beauty by Glenn & Keith. |
June 13, 2008
I had the good fortune of spending 4 days with John Mankameyer at his home and studio in Miles City, Montana.
He's located deep in the heart of cattle country! On the trail Lewis and Clark followed when exploring in the early 1800's. Near the site of Custer's Last Stand by the Little Big Horn.
John has been making crystalline glazed porcelain since the mid 1970's. After years of doing the show circuit in Northern California now he's retired and still actively experimenting with these glazes and his unique twist to them. John has a motto posted on his PC which reminds him of his charter (I guess) which reads: "I am trying to do more than make a pot with colored blotches on it"
Agate - Inspiration For John's Crystalline Glaze | Select Photos From My Visit |
Fort Keogh Livestock and Range Research Laboratory |
Montana Landscape |
June 7, 2008
I'm off to spend a week with John Mankameyer. |
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June 5, 2008
A fantastic birthday present from Avril Farley. |
May 31, 2008 72nd Firing Results
3 types of crystals |
1, 3/4, 1/2, 1/4 & 0% MnO2 in NFU in rear. |
The kitchen is going in the studio. Soon I'll be setup for visitors. |
May 29, 2008 71st Firing Results, 12" Diameter X 14 1/2" Tall
May 27, 2008
70th Firing Results |
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71st Firing Setup |
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An all Klinsky event. |
May 26, 2008
70th Firing Setup |
One coat of wood filler. |
David Turner's latest big bowl is on the bottom. It is all NFU except for the inside bottom which is 8% rutile base. The top shelf is all NFU too. I gave the pieces a heavy coat of glaze right around the top lips this time to try and get more of the action I've seen around the bottoms further up the pots. The little guys are on their second firing with a little more glaze.
On Memorial Day, the flag should be hung at half-staff until noon, when it should be raised to the top of the staff. |
May 25, 2008
May 23, 2008
Replacing elements. I used the the "B Tank" torch to bend the leads around the posts as well as bend the coils in the corners to get them to lay in the slots. I should have stretched them to about 74" length first to put them in compression a little. I'm sure they'll settle in after the first firing.
May 20, 2008 69th Firing Results
When I got home from the rock pile last night the kiln was still going through the last holds. It did shut off and was cooling, but by "Pumpkin Time" it was still 500°C. I was able to peek and saw it was not good. The crystals looked nice, but the pot had collapsed. I knew those 2 real wet rings on the outside, when I glazed the inside, were the sign of doom!
I did check into what capability my controller has, but unfortunately I didn't order the amp check feature. I plan to do a continuity and resistance check before the next firing, but I have to admit I loaded a bisque this morning.
May 19, 2008
At 8:00am this morning the cycle should have been 1/2 way through the 9 hours worth of holds. It hadn't even reached top end of 1290°C yet. The programmer was calling for 1257°C but the chamber temperature was only 1240°C. I added some more insulation to the lid and left for work. Then at 11:00am I returned and saw it had topped out and was at 1143°C on its way down to the first hold at 1000°C. It appears to be 8 hours behind schedule.
May 18, 2008
69th Firing Setup |
Cones 9 (left) thru 11 (right) from the last firing |
The Freshman Formal Dance was Friday. Kat got all dolled up and looked like a beautiful woman. |
It looks like my elements are about done. I was expecting to see an over firing condition when they got to the point of not having enough "snot" to get there (resistance too high) in the programmed time, resulting in a heck of a lot more heat work happening as it slowly, I mean slowly, crept up to top temperature. It looks to me like they are running out of gas as the furnace hit somewhere between ^12 and ^13. I didn't really pay attention but seem to recall the programmer said this cycle took 32 or 33 hours - about 10 hours longer than it should have.
I decided to fire the 69th anyway and watch it (as much as I could). I turned on the 16 segment feature (see firing schedule of April 27, 2008), pressed the start button about 6pm and noticed at about 9:30pm the programmer was calling for 500° but the chamber temperature was 495°C.
After Dance Party Note: We had about 250+ kids here for a party which ran from ~10:15pm (after the dance) until 3:30am (when I started asking people to leave). It was in the barn, the house, the yard and the Christmas Tree Field. It was like Woodstock. Driving rain all night, and mud all around the bonfire. The kids seemed oblivious too it and I imagine had a great time. I have spoken with no angry parents, neighbors, police or attorneys either.
May 14, 2008 68th Firing Results
The big one and little one in the front are first fires with one even coat (I'm happy to see) of "thick shake" glaze. A little more glaze on top and I think they would have the exaggerated growth low temperature crystals all over them. I haven't seen these crystals grow this large before. There was very little run off to the catchers, but some. Next trial I will add a little more glaze right around the top.
May 12, 2008
Two test tiles and four re-fire pots - three of which are going back in. |
More glaze with 4% CMC and thick shake consistency. |
May 11, 2008
May 10, 2008
67th Firing Setup | Norma's last piece |
Hold Temps |
Minis by Graeme Anderson, down in the land of opals. |
This load is all re-fires. I mixed more NFU with 4% CMC. The thick shake consistency made it easy to apply a reasonable coat which stayed put. There is also a test tile strip with 1, 2, 3, 4 and 5 coats of NFU to see if I can get a clearer picture of the relationship of low temperature crystal growth habit to glaze thickness. There is another with 1, 1 3/4, 2 1/2, 3 1/4 and 4% rutile.
May 8, 2008
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This is the firing schedule for the last firing. Many people have asked about it so I put it on my firing schedules page as well as here.
Jesse Hull wrote "You said, "It seems the thickness of this glaze at these low temperatures has a major impact on whether these crystals will form and grow." If you're going to compare glaze thickness -or anything else for that matter- shouldn't you use similar, if not identical, forms? The form on the left is a far cry from the one on the right... going from nearly flat to nearly vertical within your testing scheme. And the one in the middle has a neck which holds glaze that eventually runs onto the shoulder (replacing the glaze which is lost there), while neither of the others do."
Using identical forms and measured amounts of glaze for a glaze thickness comparison certainly would be a good way to quantify the situation. Maybe besides cutting into the piece to measure the glaze thickness there is an optical method to use.
I think these recent pots are examples of ones with glaze on the thin side and ones which have this type of crystal. My observation about "...the thickness of this glaze at these low temperatures..." is based:
1) On seeing the pot on the right with broadly separating rings on its top which formed at temperatures below 1000°C. And on the shoulder where it is thicker, and the high temperature crystals (1050°C to 1080°C) grow quickly there is little separation between the low temperature bands.
2) This glaze appears green when thick and tending towards aqua when thin. This thick - thin is based on believing I know how much I've brushed on.
3) Seeing these greenish pieces not having formed crystals at these low temperatures and knowing I brushed on a very heavy application of glaze.
4) Re-firing the piece, seeing the glaze flow off the pot and accumulate in the catcher, the color change towards aqua and crystals forming.
I think the piece on the right exhibits a greener color on the bottom where the glaze is thick and has small crystals with more of a traditional look, and tends toward aqua color on the top where the glaze is thin and has larger, faster growing crystals on top where the glaze is thin.
It's interesting to note though that I may say fast or slow, but the "fast" growing ones here in this "thin" glaze at these low temperatures (860°C to 1000°C) only grow at a rate of ~1inch in 9 hours. That should be enough time to grow 6" diameter crystals at higher temperatures (1080°C)
May 7, 2008 66th Firing Results (Probably the lightest load since firing #9)
May 6, 2008 (My 52nd Birthday)
66th Firing Setup |
Striking for 1/2 hour at 815°C |
Before and After (Ick!) |
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Bottles by David Snair |
May 5, 2008 65th Firing Results
These were fired with 1050°C and 1080°C holds. Click the photos for more info.
May 4, 2008 65th Firing Setup
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Thanks Kat!
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